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Draw the water: Using a 3 mL syringe, draw 2 mL of bacteriostatic water

Close examination of products derived from the reaction of UA with NO, by means of liquid chromatography-mass spectrometry (LC-MS), revealed that the dominant end-product has a molecular mass of 127 u and a chromatographic retention time of about 6 minute (Figure 2A)

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The variation in digestibility across samples indicates that the choice of defatting solvent plays a critical role

10.1016/S0167-7799(97)01076-7 59 GoutP