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Synthesis and Characterization of Diketopiperazine Derived From AX Sodium AX (19 mg, 0.05 mmol) and DTT (15 mg, 0.1 mmol) were dissolved in 1.5 ml of degassed H 2 O under N 2 atmosphere and stirred overnight at room temperature

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Dietary intervention and diet lead-in A registered dietician instructed participants on the TLC diet